You can not select more than 25 topics
Topics must start with a letter or number, can include dashes ('-') and can be up to 35 characters long.
4.6 KiB
4.6 KiB
检验鉴定系统 -- 数据文件解析方式
20240415
毛发案件
使用的仪器
沃特斯
源文件表头意思
# Name ID RT Quan Trace Area 1?Trace 1?Area
1?Ratio (Actual) 1?Ratio (Pred) 1?Ratio Flag %Dev
Primary Flags ng/mL Std. Conc 2?Trace 2?Area
2?Ratio (Actual) 2?Ratio (Pred) 2?Ratio Flag
Name -> 数据流水号，目前也存储在数据库表b_test_record_sampledata.name ，存储该字段的原因是因为在实验中一个检材可能取两次数据，方便生成检验记录表时，给检材加标识 -1、-2 等
ID -> 这个字段可能有检材、标准品、空白溶液等。标准品在文件中的标识是 STD、检材的标识是系统中检材的受理编号、质控溶液的标识 QC 、空白溶液的是 BLK、 ACN 是用来清洗针管等
RT -> 数据文件中保留时间字段
Quan Trace 和 1?Trace -> 定性离子对
Area 和 1?Area -> 峰面积
1?Ratio (Actual) -> 离子丰度比，其计算公式是 1?Area / Area
1?Ratio (Pred) -> 对比的标准品离子丰度比
1?Ratio Flag -> 标记是否检出， YES 未检出 NO检出
ng/mL -> 检材或者标准品浓度
余下的字段目前未用到
NPS案件
使用的仪器
岛津
源文件字段意思
[Header]
Data File Name D:\20231019山西临猗\2023-76-4_8.qgd
Output Date 2023/10/27
Output Time 9:39:02
[File Information]
Type 数据文件
Generated 2023/10/24 18:45:06
Generated by Admin
Modified 2023/10/27 9:39:02
Modified by Admin
[Sample Information]
Operator Name Admin
Analyzed 2023/10/24 18:52:13
Type 未知物
Level 1
Sample Name 4号毒品疑似物
Sample ID 2023-0072-1
ISTD Amount 1 1
ISTD Amount 2 1
ISTD Amount 3 1
ISTD Amount 4 1
ISTD Amount 5 1
ISTD Amount 6 1
ISTD Amount 7 1
ISTD Amount 8 1
ISTD Amount 9 1
ISTD Amount 10 1
ISTD Amount 11 1
ISTD Amount 12 1
ISTD Amount 13 1
ISTD Amount 14 1
ISTD Amount 15 1
ISTD Amount 16 1
ISTD Amount 17 1
ISTD Amount 18 1
ISTD Amount 19 1
ISTD Amount 20 1
ISTD Amount 21 1
ISTD Amount 22 1
ISTD Amount 23 1
ISTD Amount 24 1
ISTD Amount 25 1
ISTD Amount 26 1
ISTD Amount 27 1
ISTD Amount 28 1
ISTD Amount 29 1
ISTD Amount 30 1
ISTD Amount 31 1
ISTD Amount 32 1
Sample Amount 1
Dilution Factor 1
Vial# 5
Injection Volume 1
Injection Count 1
Bar Code
[Original Files]
Data File D:\20231019山西临猗\2023-76-4_8.qgd
Method File D:\20231019山西临猗\海洛因方法+数据处理.qgm
Batch File D:\20231019山西临猗\2023-1026-test.qgb
Report Format File
Tuning File C:\GCMSsolution\System\Tune1\20231024-N-#1.qgt
[File Description]
[MS Quantitative Results]
# of IDs 4
ID# Name Type ISTD Group# Mass Ret.Time Start Time End Time A/H Area Height Conc. Mode Peak# Std.Ret.Time Calibration Curve 3rd 2nd 1st Constant Ref.Ion Area Ref.Ion Height Ref.Ion Set Ratio Ref.Ion Ratio Recovery SI Ref.Ion1 m/z Ref.Ion1 Area Ref.Ion1 Height Ref.Ion1 Set Ratio Ref.Ion1 Ratio Ref.Ion2 m/z Ref.Ion2 Area Ref.Ion2 Height Ref.Ion2 Set Ratio Ref.Ion2 Ratio Ref.Ion3 m/z Ref.Ion3 Area Ref.Ion3 Height Ref.Ion3 Set Ratio Ref.Ion3 Ratio Ref.Ion4 m/z Ref.Ion4 Area Ref.Ion4 Height Ref.Ion4 Set Ratio Ref.Ion4 Ratio Ref.Ion5 m/z Ref.Ion5 Area Ref.Ion5 Height Ref.Ion5 Set Ratio Ref.Ion5 Ratio Ret. Index S/N Unit Description Threshold Tailing Ref.Ion1 S/N Ref.Ion2 S/N Ref.Ion3 S/N Ref.Ion4 S/N Ref.Ion5 S/N ISTD Name ISTD Area ISTD Height ISTD Ret.Time Noise
1 Heroin 目标物 1 327.00 10.727 10.640 10.950 1.970 142994 72693 0.00000 Auto 4 10.695 线性 0 0 0 0 0 0 0 0.00 0.00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 521.57 ppm 0.00000 1.126 139.374
2 Heroin 目标物 1 369.00 10.726 10.680 11.170 1.950 93699 48039 0.00000 Auto 9 10.695 线性 0 0 0 0 0 0 0 0.00 0.00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1010.38 ppm 0.00000 1.119 47.545
3 Heroin 目标物 1 310.00 10.665 10.630 10.675 2.200 130 59 0.00000 Auto 13 10.695 线性 0 0 0 0 0 0 0 0.00 0.00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 1.32 ppm 0.00000 -- 44.735
4 Heroin 目标物 1 268.00 10.727 10.640 11.085 1.960 93834 47994 0.00000 Auto 18 10.695 线性 0 0 0 0 0 0 0 0.00 0.00 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 648.39 ppm 0.00000 1.115 74.020
[MC Peak Table]
Type -> 表明是标准品还是要检测的样品， 未知物 待检测的样品，Standard 标准品
Sample Name -> 检材样品的名称
Sample ID -> 检材样品的编号
Name -> 所要检测的化合物名称
Mass ->本次检测的质荷比